Refining Scrap Silver with Nitric Acid

Пікірлер: 49

  • @TheGoldmansChannel
    @TheGoldmansChannel2 жыл бұрын

    G'day everyone! For those that are interested, I received the XRF results from Grappys Gold Buyers in Maryborough last night. He gave me 2 readings which I assume were from each side of the silver melt. 99.69% and 99.96%! Bloody stoked. Thanks again to Mick and Erin from Grappy$ for being Bloody champions as usual.

  • @heinzdeboer2250

    @heinzdeboer2250

    Жыл бұрын

    fantastic! Ifmay ask. At what temperature do you keep nitric solution when dissolving the silver?

  • @TheGoldmansChannel

    @TheGoldmansChannel

    Жыл бұрын

    @@heinzdeboer2250 Thanks for watching Heinz! I hope you enjoyed it. I'm not certain there's a "one temperature suits all" type answer for that one. As I'm sure there's a number of factors that would determine to most efficient temperature to keep the solution during the dissolving process. However, it seemed to me that it was more of a simmer than a boil. Too hot will drive off the distilled water too quickly. My hotplate was set on roughly medium. 2.5-3/5. Hope that helps, all the best!

  • @jimcatanzaro7808

    @jimcatanzaro7808

    7 ай бұрын

    Good job i wish you could write out exactly what you did i have pounds of silver contacts and all tested heavily with silver I already have all my acid and lab equipment ready I just don’t want to screw it up

  • @TheGoldmansChannel

    @TheGoldmansChannel

    7 ай бұрын

    Much copper mixed in with your contacts? Ideally removing all copper and just having the silver contacts would be best. I'd start with just a few of your contacts. Make up a small batch of dilute nitric and see how you go. Getting good at refining is a real experimentation process. I'm by no means close to being an expert, but i am getting better at these experiments slowly over time by trial and error. Start small, see how you go!

  • @EssexSilvering
    @EssexSilvering3 ай бұрын

    Great video, I enjoyed watching that, thanks for sharing.

  • @TheGoldmansChannel

    @TheGoldmansChannel

    3 ай бұрын

    Thanks mate! Im glad you enjoyed it. 😁 Just remember please, the video only displays my own experiments and is not meant as a tutorial for others. I made many mistakes, and still do 😊

  • @EssexSilvering

    @EssexSilvering

    3 ай бұрын

    @@TheGoldmansChannel I did the same as you at my home, was very educational and I enjoyed doing it, I to made mistakes but you learn fast 👍

  • @MrRickeyH
    @MrRickeyH2 жыл бұрын

    Good video Bryan. Commentary was good.

  • @TheGoldmansChannel

    @TheGoldmansChannel

    2 жыл бұрын

    Thanks Rick! Much appreciated. I was really happy with the 3rd attempt. I'll pop in and show it to you when I see you next

  • @jethrodigger
    @jethrodigger2 жыл бұрын

    good vid bryan. radio voice over is spot on.

  • @TheGoldmansChannel

    @TheGoldmansChannel

    2 жыл бұрын

    Thank you Jethro. Finally starting to get the hang of it. Just need to find some good gold to show off now 😁

  • @mk2ghia1976
    @mk2ghia19762 жыл бұрын

    Loved this vid! Good work. Very interesting

  • @TheGoldmansChannel

    @TheGoldmansChannel

    2 жыл бұрын

    Thanks Boothy! Glad you liked it man, hope some of the refining stuff I've been doing lately makes a bit more sense now. I'm slowly piecing it all together haha

  • @sambarhuntsman4149
    @sambarhuntsman41492 жыл бұрын

    Good watch Hayne very well put together 👍🏻

  • @TheGoldmansChannel

    @TheGoldmansChannel

    2 жыл бұрын

    Thank you Mr Huntsman. I'm slowly getting better at the movie making side of things. Audio control is my biggest focus now. Some of my earlier vids were acoustic atrocities haha

  • @kaynefryday6637
    @kaynefryday6637 Жыл бұрын

    Happy Easter to you to 😂

  • @hotrod47944
    @hotrod479443 ай бұрын

    If you were to put a piece of Steel into that waste copper nitrate solution, the copper would fall out of solution, and you could melt that down too…

  • @jimcatanzaro7808

    @jimcatanzaro7808

    3 ай бұрын

    You need to do a few more steps as well to refine the copper and the cost of materials you will lose money I just save mine in buckets for use in my silver cell as a starter solution

  • @frezhunter
    @frezhunter11 ай бұрын

    Are you using distilled water in the first part where you melt down the silver and pour it to make bbs?

  • @TheGoldmansChannel

    @TheGoldmansChannel

    11 ай бұрын

    I'm using rain water for that part Frez. Distilled water would be important for anyone who only has access to chlorinated tap water, though. Great question! I didn't event think about it at the time. 👍🏿

  • @hitandmissprospecting3833
    @hitandmissprospecting38332 жыл бұрын

    Hi mate hope you don’t mind me asking but what qualifications do you have? Based on the voice over I would assume your an electrician.

  • @TheGoldmansChannel

    @TheGoldmansChannel

    2 жыл бұрын

    I got my qualification from the University of Deez. 🤣

  • @-r-495
    @-r-495 Жыл бұрын

    Is Borax readily available or are there questions like with the nitric acid? In Europe I have not found it ti be as easy as in the US to procure these two reagents.

  • @TheGoldmansChannel

    @TheGoldmansChannel

    Жыл бұрын

    Borax is available anywhere and everywhere here in Australia. Used for many different things, like you mentioned in your previous comment. If you struggle to find it, perhaps google different general uses for it and find a product that goes by a different name but is still STB. I'm unsure what the laws are here in Aus for the purchase of Nitric, Muriatic is easily purchased in lots of places but I can't find any info on whether we need permits or something to get Nitric. Mine comes from a friend of a friend, so I've never even had to pay for it. I'm very lucky in that regard. Thanks for watching and dropping comments Mr. Cheerful. 😁

  • @jimcatanzaro7808
    @jimcatanzaro78083 ай бұрын

    Sugar and lye is faster and more pure in my experiences

  • @prospectorpete
    @prospectorpeteАй бұрын

    Great video mate. You sound Australian, where are you located

  • @TheGoldmansChannel

    @TheGoldmansChannel

    7 күн бұрын

    Thanks Pete, I am yes. I'm down in Vic 👍🏿👍🏿

  • @charlesdarwinabella6962
    @charlesdarwinabella69628 ай бұрын

    Does silver produce white bubbles instantly when nitric acid is dropped?..i have this piece and i am hoping it to be silver..it does leave a white yellowish residue after applying nitric acid..soaked another piece and it left a brown to black something attcahed to it, which is removable though..thanks!

  • @OfficiallyRetired

    @OfficiallyRetired

    5 ай бұрын

    have you found out what it is? I'm having the same problem

  • @CRaz35
    @CRaz35 Жыл бұрын

    So do you leave the heat on when your letting the silver connect to the copper

  • @TheGoldmansChannel

    @TheGoldmansChannel

    Жыл бұрын

    No heat while cementing out the silver with the copper bar. Takes quite a while, just leave it there for a few days to do its thing. 👍🏿👍🏿

  • @CRaz35

    @CRaz35

    Жыл бұрын

    Thank you

  • @daviddindal8409
    @daviddindal8409 Жыл бұрын

    Looks like it wasn't stired really well

  • @TheGoldmansChannel

    @TheGoldmansChannel

    Жыл бұрын

    A magnetic stirring hotplate would be ideal for this. But you can still do it no issues without one. Just takes a little longer 😁

  • @BEMetalMelting
    @BEMetalMelting Жыл бұрын

    Cool video but I came here specifically to see how to filter it 😂😂 any tips?

  • @TheGoldmansChannel

    @TheGoldmansChannel

    Жыл бұрын

    It's a slow process with my little system, but I just use a Buchner funnel with 100mm qualitative filter paper and slow gravity filter the solution. Ill get a vacuum pump and Buchner flask one day in future also. Once I step up my gold refining game. I only really refine silver for use with inquarting gold, to remove the excess silver from the gold so I can refine it properly without running into dramas with silver chloride. Hope that helps

  • @BEMetalMelting

    @BEMetalMelting

    Жыл бұрын

    @@TheGoldmansChannel hmm where can you find those filters?

  • @TheGoldmansChannel

    @TheGoldmansChannel

    Жыл бұрын

    @@BEMetalMelting Any lab supply companies online will have them if you search "Qualtitive filter papers". They can be folded for use with a standard conical funnel, but a Buchner funnel makes its much easier if you've got the money spare for one.

  • @TheGoldmansChannel

    @TheGoldmansChannel

    Жыл бұрын

    Sorry, Qualitative is the correct spelling

  • @BEMetalMelting

    @BEMetalMelting

    Жыл бұрын

    @@TheGoldmansChannel sweet thank you man, I’m gonna try to purify some silver this weekend that’s really the only thing I’m missing.

  • @jamescball55
    @jamescball554 ай бұрын

    H2NO3 really?

  • @TheGoldmansChannel

    @TheGoldmansChannel

    4 ай бұрын

    You know what it was meant to say don't you? Some countries don't allow citizens to access it. So we need to be careful about what chemicals I mention. I found out the other day, in some places folks can't even buy borax! What a world we live in.

  • @jimcatanzaro7808
    @jimcatanzaro78087 ай бұрын

    U need some ceramic fiber

  • @TheGoldmansChannel

    @TheGoldmansChannel

    7 ай бұрын

    Got some, building new furnaces with it soon hopefully 🤞