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Synthesis of 3,5-Dimethylpyrazole

In this video I follow the procedure in Vogel's practical organic chemistry on the synthesis of 3,5-dimethylpyrazole by the condensation of hydrazine with acetylacetone.
Correction: When I listed the melting point range for the product from the chloroform extraction I said 105 to 1-O-10 C when I meant 105-110 C
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Пікірлер: 27

  • @alex-mzlzl
    @alex-mzlzl27 күн бұрын

    This channel is very underrated

  • @jamesg1367
    @jamesg13673 жыл бұрын

    Nice photography. Great presentation. And a lesson: More ether, not less, is the Answer to Life and Everything.

  • @johnathancorgan3994
    @johnathancorgan39943 жыл бұрын

    This was great. I really wish that more amateur chemistry videos had your attention to detail, narrative style, and photography/editing. An improvement would be to add more of the theory behind the reaction and its mechanism.

  • @samira.8919
    @samira.89193 жыл бұрын

    These videos are a joy to watch!

  • @ELEKTRON1
    @ELEKTRON12 жыл бұрын

    pro-tip: use hot water for crystallization. It dissolves brilliantly in boiling water. After cooling to room temperature, the solubility drops to 31 g / dm3, you can use the refrigerator. the crystalline mass is transferred to a filter funnel. colorless crystals similar to naphthalene are obtained after filtering and washing with a little cold water. all the yellow color remains in the liquid. The filtrate can be concentrated again by heating it to below boiling point and recrystallized again. The crystals should then be dried by gently heating or in a desiccator.

  • @Jayko30
    @Jayko303 жыл бұрын

    verry well done.

  • @SetTheCurve
    @SetTheCurve2 жыл бұрын

    I got a degree in chemistry and a degree in computer science, and often wonder why. I can’t make anything truly useful that I couldn’t just buy for much less time commitment. It would be nice if someday someone would make something that seemed useful.

  • @anax22

    @anax22

    2 ай бұрын

    this is a very important nitrification inhabitor It's the sustainable future of agricultural unless we want to fuck the planet more than it's fucked

  • @dr.muhammadnasrallah298
    @dr.muhammadnasrallah2989 ай бұрын

    excellent

  • @daveedcapitan5854
    @daveedcapitan58542 жыл бұрын

    Nice job Could you please explain about 3,5 decarboxylated synthesis?

  • @achwaqachwaq305
    @achwaqachwaq3052 жыл бұрын

    Hi Can you please synthitis a pyrrol of hantzsch and pal knorr.

  • @anax22
    @anax222 ай бұрын

    hello, if i have hydrazine hydrate, how much to use and do i need water ond NaOH ?

  • @xspeeder2009
    @xspeeder20092 жыл бұрын

    Could you supply me with the book pdf or experiment of preparing 3,5 dimethyl phenol

  • @rahulkhakhriya3038
    @rahulkhakhriya3038 Жыл бұрын

    I recently read a paper in which Methyl Ethyl diketone is used. That process seems very simple but I didn't find Methyl Ethyl diketone anywhere even mentioned on internet. Can you explain how that is possible?

  • @mikemike-qx2ue

    @mikemike-qx2ue

    Жыл бұрын

    That chinese patent is naming wrong, it is their way of saying acetylacetone (2,4 pentanedione)

  • @sipitbelo3690
    @sipitbelo36902 жыл бұрын

    This was great, but i have a question, 3,5 dimethylpyrazole very soluble in water, so why we extract the ether layer? Why don't we extract the aqueous layer since the product soluble in water? Hope you'll help me to understand this

  • @karthi6990

    @karthi6990

    2 жыл бұрын

    me too have same doubt. if you find it pls share

  • @yogi5752

    @yogi5752

    Жыл бұрын

    Usually organic compounds are more soluble in organic solvents. Hence it goes to organic layer. But some portion of it also goes to water layer. So do multiple extraction. If you want to send it to the water layer add dil. HCl and extract. Then collect aqueous layer. Neutralize it. Again do extraction.

  • @user-wo2ut3iy4e
    @user-wo2ut3iy4e8 ай бұрын

    احتاج هذا كتاب

  • @mausami773
    @mausami773 Жыл бұрын

    Could u just tell us name of book ,

  • @daminitripathi7968
    @daminitripathi79683 жыл бұрын

    👍

  • @bharatchauhan7006
    @bharatchauhan7006 Жыл бұрын

    What the name of book

  • @farahaleya7985
    @farahaleya7985 Жыл бұрын

    May i know why we have to immerse it on the ice bath

  • @EddieTheH

    @EddieTheH

    Жыл бұрын

    To keep it cold! 😁

  • @user-nw3mw7dr9n
    @user-nw3mw7dr9n9 ай бұрын

    Hello, is it possible to contact you through WhatsApp?