Gold Aqua regia dissolving. Chloroauric acid. gold refining recovery. Pure gold precipitate.

Ғылым және технология

‪@MakeGold‬ aqua regia gold recovery
Aqua regia is primarily used to produce chloroauric acid, the electrolyte in the Wohlwill process. This process is used for refining the highest quality (99.999%) gold.
Aqua regia is also used in etching and in specific analytic procedures. It is also used in some laboratories to clean glassware of organic compounds and metal particles. This method is preferred over the "traditional" chromic acid bath for cleaning NMR tubes, because no traces of paramagnetic chromium can remain to spoil spectra. While chromic acid baths are discouraged because of the high toxicity of chromium and the potential for explosions, aqua regia is itself very corrosive and has been implicated in several explosions due to mishandling.
Due to the reaction between its components resulting in its decomposition, aqua regia quickly loses its effectiveness (yet remains a strong acid), so its components are usually only mixed immediately before use.
While local regulations may vary, aqua regia may be disposed of by careful neutralization, before being poured down the sink. If there is contamination by dissolved metals, the neutralized solution should be collected for disposal.
Chloroauric acid is an inorganic compound with the chemical formula HAuCl4. Both the trihydrate and tetrahydrate are known. It is an orange-yellow solid, a common precursor to other gold compounds and an intermediate in the purification of gold metal. Both the trihydrate and tetrahydrate are available commercially.
aqua regia refine gold refining recovery 24k pure 999 fine bullion ingot gold refining recovery. Pure gold precipitate produced by the aqua regia chemical refining process.
Gold Aqua regia dissolving. Chloroauric acid. gold refining recovery. Pure gold precipitate.

Пікірлер: 142

  • @MakeGold
    @MakeGold4 жыл бұрын

    Aqua regia is a very strong acid formed by the combination of concentrated nitric acid and concentrated hydrochloric acid, both of which are strong acids. It is generally used to remove metals like gold and platinum from substances, especially in microelectronics and micro-fabrications labs. Aqua regia formula and recipe Since aqua regia is just a mixture of two strong acids, it doesn’t have a chemical formula of its own. However, it can be represented as HNO3+3 HCl, which basically indicates that it’s a mixture of nitric acid (HNO-3) and hydrochloric acid (HCl). Aqua regia solution is usually a yellow, reddish-orange, fuming liquid and has a rapidly changing composition. The traditional aqua regia solution is comprised of a 3:1 molar mixture of hydrochloric acid and nitric acid, respectively. Note that concentrated nitric acid is about 65% and concentrated hydrochloric acid is nearly 35%, so the volume ratio is generally 1 part of concentrated nitric acid to 4 parts of concentrated hydrochloric acid. Another important precaution to consider is that one should add nitric acid to hydrochloric acid, and not the other way round. Usually, they make around 10 milliliters of aqua regia for experimental purposes in labs. Needless to say, since we are dealing with very strong acids here, participating chemists should wear proper protective lab gear and the apparatus should be handled with the utmost care, as aqua regia is highly corrosive. It releases toxic fumes and is very dangerous if it comes in direct contact with human skin. How does aqua regia dissolve gold? Aqua regia is primarily popular for its ability to dissolve gold, palladium and platinum, all of which don’t react easily with chemicals. Aqua regia uses and applications Since aqua regia can completely dissolve gold, it’s used to produce chloroauric acid, which, in turn, is used as the electrolyte in a process for purifying the highest quality gold. Aqua regia is also used for metal etching and cleaning lab equipment (especially glassware of organic compounds). Aqua regia is an integral part of the extraction and purification processes of gold and platinum. Aqua regia and its World War 2 story Back in 1940, when Hitler-led Germany invaded Denmark, Hungarian chemist George de Hevesy dissolved the Nobel Prize gold medals of Max von Laue and James Franck in aqua regia to keep them safe from the Nazi troops who were ransacking the chemistry lab at the Niels Bohr Institute.

  • @thole4343

    @thole4343

    4 жыл бұрын

    A

  • @sohaibal-arefi5397

    @sohaibal-arefi5397

    4 жыл бұрын

    If the concentration of nitric acid is about 68%, and the concentration of hydrochloric acid is about 32%, so what is the volume ratio of the aqua regia mixture should be?

  • @anupram3884

    @anupram3884

    2 жыл бұрын

    Hamen rhodium Pani Mein Se gold nikaalne ki rhodium nikaalne ki ful jankariyan chahie aur kya kya chemical dalta is jankariyan chahie

  • @rahimpartovi2110

    @rahimpartovi2110

    10 ай бұрын

    @@sohaibal-arefi5397 it must be 4. To 1as i see from one of the web page .

  • @momisvargas
    @momisvargas7 жыл бұрын

    This is the best video related to purifying gold.

  • @arnedalbakk6315
    @arnedalbakk63152 жыл бұрын

    Thank you fore a Great clip 😊. You are truly one of the best on KZread 🙏

  • @TheDirtydisaster
    @TheDirtydisaster Жыл бұрын

    My favorite thing about these videos from you guys is the lack of both information and entertainment.

  • @josephpecoul6532
    @josephpecoul65324 жыл бұрын

    Your gold is always very beautiful thanks for sharing.

  • @vishnudass5902
    @vishnudass59022 жыл бұрын

    A mixture of HCL and HNO3 Amazing video

  • @davidgustavomacedo1038
    @davidgustavomacedo10383 жыл бұрын

    Parabéns pelo ressultado; Deus abênçoa.

  • @azoozahmed887
    @azoozahmed8873 жыл бұрын

    Thank you, sir, for all the information, and I hope you made a video about determining the concentration of gold in the ore by titration

  • @GilsonSantos-lz4ec

    @GilsonSantos-lz4ec

    8 ай бұрын

    Senhor é um flademonio antigo chamado flabaal está escrito na bíblia Jerusalém

  • @hugogonzales8721
    @hugogonzales87214 жыл бұрын

    Can you send me a list of equipment that you used. Including the the cauldron.

  • @MarcosAurelio-eg8um
    @MarcosAurelio-eg8um4 жыл бұрын

    Congratulations for your channel I really would like to know more about this process des already thank you thanks I'm Brazilian send me your link

  • @keefardin612
    @keefardin6124 жыл бұрын

    not to well explained like how did you get to the powder gold stage I KNOW HOW but a newbie wouldnt like it tho how much was the final weight?

  • @MonkeyDAlfred
    @MonkeyDAlfred7 жыл бұрын

    Nice FF15 soundtrack

  • @TahirKhan-ko5nq
    @TahirKhan-ko5nq2 жыл бұрын

    Very nice video 😍

  • @sekkk8284
    @sekkk82844 жыл бұрын

    Aqua regia filter get water then mix urea and sodium metalbisulfite filter then get the material and then burn....lovely gold

  • @psychosorcery9923
    @psychosorcery99234 жыл бұрын

    Nice work bro i had some quest regarding to it..??

  • @Praptoprapti2023
    @Praptoprapti20232 жыл бұрын

    So this aqua regia only disolve gold? How about other impurities metal they left behid?

  • @70ssamayal69
    @70ssamayal696 жыл бұрын

    HI I HAVE ONE DOUGHT IAM ADDING MOTHERBOARD GOLD COATED PINS IN 1:2 (NITRIC AND WATER)ACID AFTER ONE HOUR I FILTRING THIS ACID IAM GETTING GREY AND ASH COLOUR DUST WITH GOLD FOILS HOW CAN IF SEPRATE GOLD AND GREY POWDER AND WHAT POWDER IS THAT HOW TO DISSOLVE

  • @TheAyhan76
    @TheAyhan765 жыл бұрын

    Aqua regia no 3to 1 /giving slowly HNO in the HCL and then failed process is give sodium sulfide when no hno in to aqua regia and then give sodium hydroxide this is good

  • @70ssamayal69
    @70ssamayal696 жыл бұрын

    IS THAT POWDER IS NICKEL

  • @andrewb7622
    @andrewb76225 жыл бұрын

    A lot of steps have been left out. Gold looks contaminated in bar form. Precipitate looked good though

  • @GilsonSantos-lz4ec
    @GilsonSantos-lz4ec8 ай бұрын

    Esse pó branco aí passar para nós internautas OK 👍

  • @kashishmishra2110
    @kashishmishra21104 жыл бұрын

    Wowww..

  • @narendrakhona1168
    @narendrakhona11682 жыл бұрын

    NOT FOR BEGINNERS. NEED MORE CAPTIONS. LOT OF STEPS MISSING.

  • @Ruban5678
    @Ruban56782 жыл бұрын

    How much gram want add metabisulfite, maximam how to dry powder final stage, r u doing heating process?

  • @gabrielgarduno7236
    @gabrielgarduno72364 жыл бұрын

    You no added Urea?

  • @sammak9281
    @sammak92813 жыл бұрын

    How to extra shine in diamonds like not properly watery colour it's some like reddish yellow and black shade in real diamond So please tell how to remove it's colour shade?

  • @keanaandkathleen1775
    @keanaandkathleen17752 жыл бұрын

    Ganyan Ang gusto ko Taga refinary ng gold

  • @skeetersaurus6249
    @skeetersaurus62496 жыл бұрын

    Ok, so what do you do if you have gold that is 'contaminated' with other metals (iron, silver, lead, etc.), where you cannot mechanically seperate them first? If you add the 'mixed metals' into Aqua Regia, you end up with impure Chloroauric Acid. If you add Sodium metabisulfite, you will precipitate more than just gold. If you preface your work by 'soaking' the mixed metals in a 10M Nitric Acid, you MIGHT get the metal purified better before making your Chloroauric Acid to start with. My question for you is, what metals DO precipitate from impure Chloroauric Acid when you add the Sodium Metabisulfite, assuming a mix in equal quantity of gold, silver (assuming amalgams of mercury also are present), tin, lead, antimony, selenium and gallium?

  • @frantiseklaluch6605

    @frantiseklaluch6605

    2 жыл бұрын

    You are right, this is pain to watch... oxalic acid is more selective... but disolve whatever with AR just hurts my eyes...

  • @shirouie

    @shirouie

    Жыл бұрын

    Sir, could you clarify the steps? How did he end up with chloroauric acid?

  • @frantiseklaluch6605

    @frantiseklaluch6605

    Жыл бұрын

    @@shirouie HNO3 oxidises gold, that reacts with HCl formig complex H(AuCl4), soluble form of gold.

  • @SunnyKetPatil

    @SunnyKetPatil

    Жыл бұрын

    How to remove tin from gold

  • @frantiseklaluch6605

    @frantiseklaluch6605

    Жыл бұрын

    @@SunnyKetPatil As for me, cupelation...

  • @kartiksaraswat7448
    @kartiksaraswat74484 жыл бұрын

    What you add water in aqua regia

  • @amolbgadkari
    @amolbgadkari3 жыл бұрын

    Can anyone help to clarify how the used chemicals are neutralised before going to drain. A video on disposal would be of great help.

  • @justabouthadit5872

    @justabouthadit5872

    Жыл бұрын

    No need to neutralize anything, just label it properly and take it to your local landfill and or hazmat facility and they take it and do the dirty work.

  • @manojkhera875
    @manojkhera8753 жыл бұрын

    U must tell how this aqua is made

  • @temesgentenaw3308
    @temesgentenaw3308 Жыл бұрын

    hey dude....to form the aqua regia we use 3 hcl by 1 nho3 ....then we add 2 gram gold in aqua regia.Can we precipitate by cu and we can get more than 2 gram au ....

  • @user-wv9nm8jg1v
    @user-wv9nm8jg1v9 ай бұрын

    Hi I need help with my gold, I did it but I failed, the sodium metabisulfite is sitting under my beaker

  • @sunilchatarpaul6190
    @sunilchatarpaul61905 жыл бұрын

    Hi I need some info can u plz help me

  • @DeepakKumar-fy9qs
    @DeepakKumar-fy9qs3 жыл бұрын

    Sir very nice

  • @GilsonSantos-lz4ec

    @GilsonSantos-lz4ec

    8 ай бұрын

    Senhor é um flademonio antigo chamado flabaal está escrito na bíblia Jerusalém

  • @masacatior
    @masacatior3 жыл бұрын

    I see you on the dark side of the Moon 🎶

  • @ismailislam3617
    @ismailislam36175 жыл бұрын

    Le nom de produie

  • @mahhamadchanda7107
    @mahhamadchanda71074 жыл бұрын

    WICH NAEM BORAX POWDEA

  • @serenity6988
    @serenity69885 жыл бұрын

    Sir I have a ? for you based on many videos I have watched and studied. Is there a new tech that allows anyone to dissolve gold with a citric acid based setup. I watched on where they dipped in cpu boards and with in 15 to 30 sec, the gold was off. No electrolysis applied in action. Very impressive and applicable more than you can imagine if true. looking for this formula for me and others. Can you help in any way.

  • @anahoae

    @anahoae

    5 жыл бұрын

    Impossible any acid used for circuit boards is to remove other materials from gold not the opposite

  • @styx7989
    @styx79896 жыл бұрын

    with 10gr of ram fingers he have 1kg of gold ^^

  • @claybutler1662
    @claybutler16624 жыл бұрын

    What's proper PH before adding metabisulfate ?

  • @deivisonmuller9933

    @deivisonmuller9933

    10 ай бұрын

    Também queria saber

  • @muhmmadrafqta6508
    @muhmmadrafqta65084 жыл бұрын

    Sir tell me the nemes of the acid to this is will be help for my life please

  • @tahsinmaria112

    @tahsinmaria112

    3 жыл бұрын

    HCI and HNO3 are used to make aqua regia

  • @vinayaknavanale7858
    @vinayaknavanale78586 жыл бұрын

    At last the powder you get --is that gold salt or pure gold. what to do to get pure gold powder ?? i need pure gold powder for medical purpose. not gold salt ??

  • @anahoae

    @anahoae

    5 жыл бұрын

    Must be gold as well as nobil metals his way may include even copper and lead

  • @ramadasprabhu7645

    @ramadasprabhu7645

    4 жыл бұрын

    Gold donot have any medicinal value

  • @pastorini59
    @pastorini594 жыл бұрын

    Is it possible to create aqua regia, instead of using nitric acid, use potassium nitrate?

  • @AmineAmine-ty6nx

    @AmineAmine-ty6nx

    3 жыл бұрын

    yes u can

  • @user-qd9gl2op8qHmada
    @user-qd9gl2op8qHmada Жыл бұрын

    اخى العزيز كيف اتجنب رائحة SMB الصعبه

  • @MakeGold

    @MakeGold

    Жыл бұрын

    use the hood or chemical protective mask

  • @loweverest548
    @loweverest5487 жыл бұрын

    Sir, does it matter or not if you neutralize the acid before dropping it with SMB?

  • @justabouthadit5872

    @justabouthadit5872

    Жыл бұрын

    The smb will have a more active reaction (foaming and boiling) if you don't neutralize first with urea, but it makes no difference in the quality of the end product.

  • @maii0082
    @maii00826 жыл бұрын

    2:44 Suddenly more liquid, what kind of liquid?

  • @TVchristezite

    @TVchristezite

    3 жыл бұрын

    Sodium metabisulfite

  • @SuperTubeFan

    @SuperTubeFan

    3 жыл бұрын

    he may have added Urea and water to neutralize excess nitric acid

  • @TahirKhan-ko5nq
    @TahirKhan-ko5nq2 жыл бұрын

    Hey what is SMB powdar you ansr Urdu

  • @marimack8578
    @marimack85784 жыл бұрын

    Can i use muriatic acid to make aqua regia?

  • @nevercertain

    @nevercertain

    Жыл бұрын

    That's what hydrochloric acid is. HCL = Muriatic acid Edit: just realized this comment was made 3 years ago but still gonna leave my reply in case anyone has the same question

  • @dursuntopcu5200
    @dursuntopcu52003 жыл бұрын

    dude bak bu böyle bir cok ceşitli ürünler elde ediyorum sonucuna veamiyorum camu ve tozlar cok var

  • @steveperez660
    @steveperez6602 жыл бұрын

    Nitric acid

  • @alisedattemel8011
    @alisedattemel8011 Жыл бұрын

    Direk olarak tuzlu suda akım ile direk elde edebilirsin au klorür içeren bir metall tuzda inorganik bir metaldir elektro şok tuzlu su direk kahverengi çökelek ekde edebilirsin ugraşma okadar

  • @qarimahmoodmiya4294
    @qarimahmoodmiya42945 жыл бұрын

    Sir sodium Kahan milega.yani kis dukan par.potassium nitrate kaha aur kis dukan par milega.kiya aasani see mil jaega????

  • @moazzamalish4682

    @moazzamalish4682

    5 жыл бұрын

    Chemical laboratory sa pata karo

  • @prashantkeshavbhagat5940
    @prashantkeshavbhagat59406 жыл бұрын

    For 10gm un pure gold how to use

  • @Hawkido

    @Hawkido

    2 жыл бұрын

    Inquart gold with silver until the gold is 25% or less. smelt, dribble alloy into water to increase surface area, remove and dry. Place in a glass beaker, Add nitric acid to remove silver and copper from alloy leaving gold (and possible lead in alloy) *the gas produced by reacting nitric acid is dangerous to breath, commonly referred to as red death, you have been warned*, the silver/copper will be carried away by the nitric acid rinse. Keep this as you can recover the Silver form this later by adding a copper sheet to the silver solution to release the silver. Once the gold alloy stops reacting with nitric acid after several rinses, then you can begin the Aqua Regia treatment, use as little nitric acid as possible to dissolve the gold by adding it slowly to the HCL/AU mixture. The gold will slowly begin to dissolve into the HCL, once it is all in solution add a few millilitres of Sulfuric Acid to cause any lead in solution to precipitate out as lead sulfides which can then be filtered out of solution. Then you can begin to precipitate the Gold out of your final product using Sodium MetaBisulfate. You can check to see if you have removed all the gold from solution by using StannousChloride on a sample drawn from the solution. Properly neutralize all acids and dispose properly depending upon your region.

  • @scruffles1132
    @scruffles11327 жыл бұрын

    What were the crystals added at 7:30?

  • @jomariecinco4655

    @jomariecinco4655

    7 жыл бұрын

    I believe it was sodium metabisulfite, to make the metal shiny.

  • @chadgilbertson3821

    @chadgilbertson3821

    7 жыл бұрын

    Or borax. Metabisulfite does the same.

  • @angelnunez1179

    @angelnunez1179

    7 жыл бұрын

    Scruffles 113 that would be... Borax.

  • @scruffles1132

    @scruffles1132

    7 жыл бұрын

    Angel Nunez TY.

  • @ahzelparaiso1648

    @ahzelparaiso1648

    6 жыл бұрын

    It could be BORAX or SODIUM NITRATE..

  • @kimmayongka-bunyan9714
    @kimmayongka-bunyan97146 жыл бұрын

    Is Aqua Regia same Cyanide? In dissolving cyanide, what is the ratio between water and cyanide? thanks a lot brother.

  • @thomasringjr.1630

    @thomasringjr.1630

    6 жыл бұрын

    Aqua Regia is a combination of Hydrochloric and Nitric acid.

  • @netofuentes8308

    @netofuentes8308

    6 жыл бұрын

    cornstarch i-$0-late- gold

  • @aridinarifi5833

    @aridinarifi5833

    5 жыл бұрын

    Bahasa Indonesia ya apa Obat cobak terangkan

  • @mr.l2871
    @mr.l28717 жыл бұрын

    👍🌟🌟🌟

  • @mostafaelbadry758
    @mostafaelbadry7585 жыл бұрын

    I fellowed the same steps and had a white powder,,,,why please?

  • @andrewb7622

    @andrewb7622

    5 жыл бұрын

    Add more HCL

  • @saidgilbygilby6397
    @saidgilbygilby63976 жыл бұрын

    متميز

  • @salihakdag6371
    @salihakdag6371 Жыл бұрын

    👍👍

  • @daneenorris5417
    @daneenorris54175 жыл бұрын

    Any other small refiners want to help each other out?

  • @andrewb7622

    @andrewb7622

    5 жыл бұрын

    What do you mean?

  • @hannible1002

    @hannible1002

    2 жыл бұрын

    Yea could we chat?

  • @johnnyleewalker9872
    @johnnyleewalker98722 жыл бұрын

    The fumes are more than Dangerous they’re deadly in more ways than one.

  • @hannible1002

    @hannible1002

    2 жыл бұрын

    Who cares if you get rich lol

  • @GilsonSantos-lz4ec
    @GilsonSantos-lz4ec8 ай бұрын

    Água régia onde devo comprar

  • @MakeGold

    @MakeGold

    5 ай бұрын

    is a mixture of nitric acid and hydrochloric acid, optimally in a molar ratio of 1:3

  • @jeffstewart8627
    @jeffstewart86275 жыл бұрын

    WRONG... In every way imaginable.

  • @bookvillage3152
    @bookvillage31524 жыл бұрын

    He is wrong he must resources the nitric acid with urea or soulfamic acid then bring sodium metabi sulfite and its dont need put sodium metabi sulfite a lot

  • @shrikantvedpathak785

    @shrikantvedpathak785

    3 жыл бұрын

    I made mistake. I put extra sodium metabi sulphite in aqua regia solution it results precipitated gold again goes in solution Please help me.. What should I do?

  • @jyotiben6723
    @jyotiben67232 жыл бұрын

    Hai

  • @haribahadurbiswa9091
    @haribahadurbiswa90913 жыл бұрын

    Like 🌹

  • @chickenj90
    @chickenj904 жыл бұрын

    That last picture isn't pure gold and probably some random stock image

  • @GilsonSantos-lz4ec

    @GilsonSantos-lz4ec

    8 ай бұрын

    Imagem do flademonio deus zeus 👹

  • @samksa802
    @samksa8025 жыл бұрын

    وين القى المواد

  • @anahoae

    @anahoae

    5 жыл бұрын

    تعتمد على البلد الذي تسكنه

  • @anahoae

    @anahoae

    5 жыл бұрын

    هناك طرق أفضل من هذه الطريقة

  • @sandorracz2401
    @sandorracz24015 жыл бұрын

    UREA??????

  • @tejas9987

    @tejas9987

    3 жыл бұрын

    No

  • @SuperTubeFan

    @SuperTubeFan

    3 жыл бұрын

    He added something just before 2:44

  • @keanaandkathleen1775
    @keanaandkathleen17752 жыл бұрын

    Walang makikialam ng ginto ko Doon sa dasmarenias salawag cavite maliban Kay mayor joey Suan sya lang puwede Dyan.

  • @steveperez660
    @steveperez6602 жыл бұрын

    You are wasting gold when it is not covered up

  • @masacatior
    @masacatior2 жыл бұрын

    See you on the dark side of Moon

  • @TheAyhan76
    @TheAyhan765 жыл бұрын

    I’m forgot Kalium hydroxide killed HNO

  • @russellangellimalima4746
    @russellangellimalima4746 Жыл бұрын

    Show

  • @abinaslimbu3057
    @abinaslimbu30572 жыл бұрын

    Earth worn

  • @MyScreenNameIsTroubledOne
    @MyScreenNameIsTroubledOne Жыл бұрын

    I mean, I respect it, but that is not “pure gold” by any stretch of the imagination. It’s gold. Yeah. But “pure gold” has meaning to it, and this is not it.

  • @johntherrian5365

    @johntherrian5365

    5 ай бұрын

    Smb will bring down 99.9x% gold if used correctly. It is rather pure.

  • @keanaandkathleen1775
    @keanaandkathleen17752 жыл бұрын

    Gobywrno kame Dito baket

  • @marcofuina9736
    @marcofuina9736 Жыл бұрын

    NON è oro puro quello.

  • @astritibrahimi4918
    @astritibrahimi49184 жыл бұрын

    24karat

  • @joehutter2071
    @joehutter20715 жыл бұрын

    I don't like it when you people make f****** videos of recovering gold and you don't talk through it you should jealous the step by step process

  • @ebrahimesawy3124
    @ebrahimesawy31247 жыл бұрын

    I'm from Egypt, I want to sell a large quantity of scrap computer is ready to work Ram and Brcissor

  • @seanandrews8217

    @seanandrews8217

    5 жыл бұрын

    Contact info want to buy

  • @msheikh3046
    @msheikh30469 ай бұрын

    Incomplete video

  • @MakeGold

    @MakeGold

    5 ай бұрын

    Hey there! Thanks for watching the video!

  • @fancyunbox
    @fancyunbox6 жыл бұрын

    fack videos

  • @styx7989
    @styx79896 жыл бұрын

    pure fake

  • @user-wv9nm8jg1v
    @user-wv9nm8jg1v9 ай бұрын

    Hi I need help with my gold, I did it but I failed, the sodium metabisulfite is sitting under my beaker

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